J. J. (edited by) Fripiat's Advanced techniques for clay mineral analysis: invited PDF

By J. J. (edited by) Fripiat

ISBN-10: 0444420029

ISBN-13: 9780444420022

Invited Contributions from the Symposium held through the seventh overseas Clay convention, Bologna and Pavia, Italy, 6-12 Sept. 1981

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Additional info for Advanced techniques for clay mineral analysis: invited contributions from the symposium held at the 7th International Clay Conference, September 6-12, 1981, Bologna and Pavia, Italy

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A c c u r a t e o r i e n t a t i o n a l o n g dense rows can t h e o r e t i c a l l y be performed by u s i n g a t i l t i n g s t a g e and c h e c k i n g by means o f t h e d i f f r a c t i o n p a t t e r n . However, owing t o t h e beams e n s i t i v i t y , t h i s method i s t o o slow t o be p r o p e r l y used f o r c l a y m i n e r a l s . The s i m p l e s t way seems t o r e c o r d images o f a g r e a t number o f p a r t i c l e s h a v i n g random azimuth; t h e p r o b a b i l i t y o f f i n d i n g d o t t e d s t r u c t u r e - i m a g e s becomes t h u s f a i r l y h i g h .

G. Lee e t a l , 1975b). - I n t e r l a y e r s o r p t i o n o f o r g a n i c compounds has been v i s u a l i z e d as shown i n F i g . 7. , e s p e c i a l l y when combined w i t h t h i n sectioning. The f i r s t s t a ges of s y n t h e t i c a l c h r y s o t i l e g r o w t h have been shown by Yada and I i s c h i (1977) i n d i f f e r e n t pH and hydrothermal c o n d i t i o n s . Layer f o r m a t i o n and s t a c k i n g f o l l o w e d b y c u r l i n g t o t u b u l a r f i b e r s c o u l d be d i r e c t l y observed on lattice-fringe images w i t h i n l e s s t h a n an hour, whereas X-ray d i f f r a c t i o n c o u l d n o t d i s c l o s e any t r a c e o f c h r y s o t i l e c r y s t a l l i z a t i o n b e f o r e one o r several days.

The majority of m a t e r i a l s , including those having i d e a l , s t o i c h i o m e t r i c c r y s t a l s t r u c t u r e s , t h e r e f o r e In c o n t r a s t , X-rays e x h i b i t only give r i s e t o both types of s c a t t e r i n g . coherent s c a t t e r i n g from p e r f e c t c r y s t a l s , incoherent o r d i f f u s e s c a t t e r i n g being a consequence of c r y s t a l l i n e imperfections o r s t r u c t u r a l d i s o r d e r ( a l l o y s , amorphous s o l i d s ) .

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Advanced techniques for clay mineral analysis: invited contributions from the symposium held at the 7th International Clay Conference, September 6-12, 1981, Bologna and Pavia, Italy by J. J. (edited by) Fripiat


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